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ProjTitle.icon 8. METHODS OF ANALYSIS AND SAMPLING

8.1.   Sampling

Sampling shall be done in accordance with the provisions of ISO 5555:2001, Animal and vegetable fats and oils Sampling.

8.2.   Analysis

To ensure compliance with this quality standard, the samples selected as specified in clause 9 shall be tested in accordance with the appropriate testing procedures:


Test parameter

Method

Determination of moisture content

  • AOAS 920.116

  • IUPAC 2.60

  • ISO 662.1998

Determination of free fatty acid
content: acid 
value and acidity
  • ISO 660.1996

  • IUPAC 2.201

Determination of relative density

  • IUPAC 2.101

Determination of saponification value

  • ISO 3657:1988 (revised 1992)

  • IUPAC 2:202

Determination of iodine value

  • AOAC 925.56

  • ISO 3961:1999

Determination of peroxide value

  • AOCS cd. 8b – 90

  • IUPAC 2501

  • ISO 3960:2005

Determination of unsaponifiable matter

  • ISO 3596-1:1996

  • IUPAC 2.401

Determination of insoluble impurities content
  • ISO 663:2000

  • IUPAC 2604

Determination of melting point

  • ISO 6321:2002

Determination of lead content (Pb)

  • ISO 12193:1994

  • AOAC 972.25

  • AOAC 994.02

  • IUPAC 2632

Determination of arsenic content (As)

  • AOAC 952.13

  • IUPAC 3136



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